Probing the Earliest Stages of Zeolite Crystallisation

DOI

Our aim is to provide new data concerning the evolution of amorphous gel phases into crystalline inorganic materials to allow information about crystallisation mechanism of solids with important applications for the future design of new materials. We have selected nanoporous zeolite materials to study as a model system, and based on some preliminary results, will study the local and medium-range order of amorphous precursor gels that have been aged for various periods. Total neutron scattering will be used to measure radial distribution in the gel phases (in the presence of their mother liquor to avoid complications on quenching) and by looking at how they evolve into the crystalline zeolite we will be able to determine how the structure of the gel affects the nature of the crystalline phase ultimately formed. The work forms the beginning of a joint STFC-Warwick funded PhD studentship.

Identifier
DOI https://doi.org/10.5286/ISIS.E.24067653
Metadata Access https://icatisis.esc.rl.ac.uk/oaipmh/request?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:icatisis.esc.rl.ac.uk:inv/24067653
Provenance
Creator Dr Alex Hannon; Dr Emma Barney; Professor Richard Walton; Dr Helen Playford
Publisher ISIS Neutron and Muon Source
Publication Year 2012
Rights CC-BY Attribution 4.0 International; https://creativecommons.org/licenses/by/4.0/
OpenAccess true
Contact isisdata(at)stfc.ac.uk
Representation
Resource Type Dataset
Discipline Photon- and Neutron Geosciences
Temporal Coverage Begin 2009-05-21T08:47:21Z
Temporal Coverage End 2009-05-24T14:22:01Z