XAFS data at Pd & In K-edges recorded in situ during reduction and ex situ.


X-ray absorption spectroscopy was performed at Diamond Light Source, UK, at B18 for the Pd/In2O3 & Pd/In2O3/Al2O3 species. Data was collected at the Pd and In K-edges in transmission mode using a QEXAFS setup with fast scanning Si(311) crystal monochromators. The time resolution here was roughly 90 seconds per spectrum. Samples were packed into an in-house custom-made capillary system designed and constructed by Diamond Light Source. 50 mg of 200-300 μm catalyst particles were packed between 3 cm of quartz wool.

DOI https://doi.org/10.5522/04/23054465.v1
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Metadata Access https://api.figshare.com/v2/oai?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:figshare.com:article/23054465
Creator Beale, Andrew; Allen, Lisa; Negahdar, Leila
Publisher University College London UCL
Contributor Figshare
Publication Year 2023
Rights https://creativecommons.org/licenses/by/4.0/
OpenAccess true
Contact researchdatarepository(at)ucl.ac.uk
Language English
Resource Type Dataset
Discipline Chemistry; Natural Sciences