We developed self-assembling peptide-based hydrogels containing two-dimensional clay nanoparticles. The clay nanoparticles are ultrathin nanomaterials having a high degree of anisotropy and functionality that results in enhanced surface interactions with biological molecules. However, due to the heterogeneous nature of these hybrid hydrogels and the contrast variation of both the peptide nanofibers and the clay nanodiscs, a technique such as SANS that will enable an accurate elucidation of the spatio-temporal orientation of the individual components constituting the bulk hydrogels is highly desirable. Therefore, we hope to measure the neutron scattering of a library of peptides and their hybrid hydrogels with clay nanoparticles.