Replication data for "A water-soluble polyphosphorhydrazone Janus dendrimer built by “click” chemistry as support for Ru-complexes in catalysis".

Bruker Topspin, 4.1.1 or higher

MestReNova, 12.0.0 or higher

OriginPro, 8.1 or higher

METHODOLOGICAL INFORMATION

1. Description of methods used for collection-generation of data: 1H NMR spectra were recorded on Agilent Mercury spectrometers (300 MHz, 400 MHz, 600 MHz). Chemical shifts (δ) are reported in parts per million (ppm) downfield from trimethylsilane (TMS) and referred to residual solvent peak: CDCl3 (δH = 7.26 ppm) or DCM-d2 (δH = 5.32 ppm). The spectra were processed using MestReNova software. 13C NMR spectra were recorded at room temperature. Chemical shifts are reported in parts per million downfield from TMS signal and referred to residual peak solvent: CDCl3 (δC = 77.2 ppm) or DCM-d2 (δC = 54.0 ppm). Otherwise stated, the multiplicity refers to 1H decoupled spectra. The spectra were processed using MestReNova software. 31P NMR spectra were recorded at room temperature in CDCl3 or DCM-d2. Chemical shifts are reported in parts per million relative to H3PO4 85% aqueous solution (δP = 0.00 ppm) as an external standard. The spectra were processed using MestReNova software. IR spectra were recorded with on a Bruker Tensor 27 spectrometer fitted with a universal Attenuated Total Reflectance Golden Gate module. Gas chromatography (GC) chromatograms were recorded on a PerkinElmer Clarus 580 model, using an IntertCap 5MS-Sil column with helium as carrier gas. High-resolution mass spectra (HR-MS) were measured at the Servicio de Espectrometría de Masas at the Universidad de Zaragoza. Elemental Analyses and Inductively coupled plasma (ICP-OES) were measured at the Servei d’Anàlisi Química de l’Universitat Autònoma de Barcelona.

2. Methods for processing the data: NMR, IR, Mass Spectra, Gas chromatography are presented Raw. Elemental analyses and ICP analyses are presented as a report from the Servei d'Anàlisi Química de la UAB. Gas chromatography are also presented as a PDF file with the summary of results per each sample.

3. Instrument- or software- specific information needed to interpret the data: NMR spectra: Bruker Topspin 4.1.1 or higher,or MestReNova 12.0.0 or higher. IR data: OriginPro 8.1 or higher, or any other graphic representation program, such as Microsoft Excel. Gas chormatography: Adobe Acrobat Reader, or any other graphic representation program, such as Microsoft Excel. ICP: Adobe Acrobat Reader, or any other graphic representation program, such as Microsoft Excel.