Structure, temporal fluctuation and vibrational spectrum of the surfactant shell of PbS nanocrystals in solution

DOI

We propose to continue the investigation of the organic surfactant shell's adsorption on colloidally stable semiconductor nanocrystals in hexane-d14 solution, the softness of this organic layer and its influence on the vibrational spectrum of the nanocrystals. PbS nanocrystals coated with oleic acid as the surfactant are technologically relevant for quantum dot-based solar cells and subject to long-term investigations by several research groups including our collaboration, utilizing electron microscopy, X-ray scattering, optical/NIR-spectroscopy, Raman spectroscopy, etc. We propose a combined approach using time-of-flight (TOF) and backscattering (NBS) spectroscopy on the same PbS nanocrystal solution to elucidate the dependence of the vibrational spectrum (using TOF) on the volume and dynamics of the oleic acid shell already measured by SANS and NBS in proposal 9-12-498, respectively. This experiment becomes feasible due to the previous complimentary characterization as well as the extremely high flux available at ILL, which is of paramount importance considering the relatively low volume fraction of the surfactant shell (approx. 1 monolayer on PbS with a diameter of 50 (±3) Å

Identifier
DOI https://doi.org/10.5291/ILL-DATA.9-10-1514
Metadata Access https://data.ill.fr/openaire/oai?verb=GetRecord&metadataPrefix=oai_datacite&identifier=10.5291/ILL-DATA.9-10-1514
Provenance
Creator Andre, Alexander; Schreiber, Frank; Scheele, Marcus; Koza, Michael Marek; Maiti, Santanu; Seydel, Tilo
Publisher Institut Laue-Langevin
Publication Year 2018
Rights OpenAccess; info:eu-repo/semantics/openAccess
OpenAccess true
Representation
Resource Type Dataset
Size 5 GB
Version 1
Discipline Particles, Nuclei and Fields