Experimental Data to the publication "Synthesis of Micro 14C-Labelled Polylactide for Environmental Assessment Analysis"

DOI

Further NMR and IR spectroscopic data, SEC data and TGA and DSC data for the ring opening polymerisation of 14C-lactide with a non toxic Zn catalyst were deposited.

GPCmax VE-2001 from Viscotek: two Malvern Viscotek T columns (porous styrene divinylbenzene copolymer) with a maximum pore size of 500 and 5000Å, a refractive index detector (VE-3580), and a viscometer (Viscotek 270 Dual Detector)

Bruker Avance II (400MHz) NMR spectrometer

Bruker Avance III (400MHz) NMR spectrometer

Shimadzu IRTracer 100 using a CsI beam splitter in combination with an ATR unit (Quest model from Specac utilizing a robust monolithic crystalline diamond)

Netzsch DSC 204 F1 Phoenix equipped with an intra-cooler

Linseis STA PT1600 with the HDSC Type S measuring unit (Pt10%/Pt-Rh) and the L75/240 RT-1600 furnace

Identifier
DOI https://doi.org/10.22000/ck37qkdet7mrfu3w
Metadata Access https://www.radar-service.eu/oai/OAIHandler?verb=GetRecord&metadataPrefix=datacite&identifier=10.22000/ck37qkdet7mrfu3w
Provenance
Creator Adeleh, Sara; Becker, Tabea ORCID logo; Herres-Pawlis, Sonja ORCID logo; Bol, Roland ORCID logo; Drewes, Birte ORCID logo; Pütz, Thomas (ORCID: 0000-0003-2101-448X)
Publisher RWTH Aachen University,Forschungszentrum Jülich
Contributor RADAR
Publication Year 2025
Funding Reference Bioeconomy Science Center financially supported by the Ministry of Culture and Science BioSC Other 313/323-400-002 13 NRW Strategieprojekt BioSC BioPlastiCycle; Werner Siemens-Stiftung WSS Other WSS-Jahrhundertprojekt catalaix
Rights Open Access; Creative Commons Attribution Non Commercial Share Alike 4.0 International; info:eu-repo/semantics/openAccess; https://creativecommons.org/licenses/by-nc-sa/4.0/legalcode
OpenAccess true
Representation
Language English
Resource Type NMR and IR spectroscopic data, SEC, TGA and DSC experimental data; Dataset
Format application/x-tar
Discipline Chemistry; Engineering Sciences; Materials Science; Materials Science and Engineering; Natural Sciences
Temporal Coverage 2024-2025