X-Ray fluorescence (XRF) of discrete samples from IODP Hole 389-M0097A

DOI

Results of X-Ray fluorescence (XRF) on discrete samples from the above given hole of International Ocean Discovery Program (IODP) Expedition 389 (Hawaiian Drowned Reefs). The offshore phase of this expedition took place between 2023-08-31 and 2023-10-31 onboard multipurpose vessel MMA Valour sailing from and to Barbers Point Harbor, Hawai'i, USA, followed by the onshore phase from 2025-02-06 to 2025-02-26 at the Bremen Core Repository (BCR) hosted at MARUM – Center for Marine Environmental Sciences, University of Bremen. During the onshore phase a set of solid-phase samples were taken from the work halves of core sections, with a volume of approx. 10 cubic centimeters each, were taken with the purpose to be later on split into aliquots for the following three analyses: X-ray diffraction, carbon and X-ray fluorescence. Bulk samples were subsequently freeze-dried, ground and homogenized to a fine powder (<20 µm particle size) by ECORD Science Operator staff using a pestle and an agate mortar or a ball mill. For elemental composition analyses an aliquot of approx. 4 g (±0.2 g) powdered and homogenized sample was weight into a plastic cuvette consisting of a Mylar foil bottom covered with polypropylene film ad compacted twice with a force of approx. 25 kg/cm3 on a plastic piston to obtain a smooth surface. Elemental concentrations were then determined by ED-XRF spectroscopy utilizing a PANalytical Epsilon 3-XLE benchtop ED-XRF spectrometer operated in the MARUM sediment geochemistry laboratory. Quality flag "#0" indicates the measurements' result was below detection limit.For further methodological information see methods chapter in Webster, J.M. et al., 2025 https://doi.org/10.14379/iodp.proc.389.2025

Data was submitted and proofread by Vera Barbara Bender, MARUM - Center for Marine Environmental Sciences (University Bremen) on behalf of ECORD Science Operator Data Management (https://www.ecord.org).

Identifier
DOI https://doi.org/10.1594/PANGAEA.986540
Related Identifier References https://doi.org/10.14379/iodp.proc.389.2025
Metadata Access https://ws.pangaea.de/oai/provider?verb=GetRecord&metadataPrefix=datacite4&identifier=oai:pangaea.de:doi:10.1594/PANGAEA.986540
Provenance
Creator Webster, Jody M ORCID logo; Ravelo, Ana Christina (ORCID: 0000-0003-3929-677X); Grant, Hannah; Stewart, Margaret S (ORCID: 0000-0002-0633-252X); Rydzy, Marisa; Le Ber, Erwan ORCID logo; Allison, Nicola ORCID logo; Asami, Ryuji ORCID logo; Boston, Brian ORCID logo; Braga, Juan-Carlos ORCID logo; Brenner, Logan; Chen, Xuefei (ORCID: 0000-0002-7789-671X); Chutcharavan, Peter; Dutton, Andrea (ORCID: 0000-0002-3836-119X); Felis, Thomas ORCID logo; Fukuyo, Naoto; Gischler, Eberhard; Greve, Sahra ORCID logo; Hagen, Amy; Hamon, Youri; Hathorne, Ed C ORCID logo; Humblet, Marc; Jorry, Stephan J ORCID logo; Khanna, Pankaj ORCID logo; McGregor, Helen V ORCID logo; Mortlock, Richard A; Nohl, Theresa ORCID logo; Potts, Donald C; Prohaska, Ana; Prouty, Nancy G ORCID logo; Renema, Willem ORCID logo; Rubin, Kenna Harmony; Westphal, Hildegard ORCID logo; Yokoyama, Yusuke ORCID logo
Publisher PANGAEA
Publication Year 2025
Rights Creative Commons Attribution 4.0 International; https://creativecommons.org/licenses/by/4.0/
OpenAccess true
Representation
Resource Type Dataset
Format text/tab-separated-values
Size 207 data points
Discipline Geology; Geosciences; Geospheric Sciences; History; Humanities; Natural Sciences
Spatial Coverage (-156.063 LON, 19.942 LAT); Hawaii, USA
Temporal Coverage Begin 2023-09-07T00:00:00Z
Temporal Coverage End 2023-09-09T00:00:00Z