Neutron scattering to characterise protein interactions with solid-liquid interfaces at different densities in bioprocessing

DOI

Objectives of this proposal aim to shed light on how adsorption processes such as protein A chromatography, used to purify biologics, affect protein propensity for aggregation. Protein A chromatography has been found to increase the aggregation rate of an IgG4 subsequently exposed to low pH. Loading a low concentration of IgG onto the resin increased aggregation rates further. Using neutron reflectivity, we wish to study the conformation of IgG4 when adsorbed to immobilised protein A. We wish to examine whether the conformation or orientation of the adsorbed molecules is affected by either the density of immobilised ligands, or the concentration of protein bound. It is hypothesised that intermolecular forces and rotational freedom affect the structural integrity of the adsorbed proteins, and their orientation in relation to the adsorbent surface, thus influencing aggregation phenomena.

Identifier
DOI https://doi.org/10.5286/ISIS.E.79107161
Metadata Access https://icatisis.esc.rl.ac.uk/oaipmh/request?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:icatisis.esc.rl.ac.uk:inv/79107161
Provenance
Creator Dr Alice Mazzer; Mr Thomas Johnson; Professor Christopher Roberts; Miss Maria Papachristodoulou; Dr Luke Clifton; Professor Daniel Bracewell
Publisher ISIS Neutron and Muon Source
Publication Year 2019
Rights CC-BY Attribution 4.0 International; https://creativecommons.org/licenses/by/4.0/
OpenAccess true
Contact isisdata(at)stfc.ac.uk
Representation
Resource Type Dataset
Discipline Biology; Biomaterials; Construction Engineering and Architecture; Engineering; Engineering Sciences; Life Sciences; Materials Science; Materials Science and Engineering
Temporal Coverage Begin 2016-05-14T08:00:00Z
Temporal Coverage End 2016-05-17T08:00:00Z