Analytical data for: <b>Nickel-Catalyzed Cross-Coupling of Aryl Chlorides by Heated Mechanochemistry: Scalable Suzuki-Miyaura Reactions via Twin-Screw Extrusion</b>

DOI

The direct use of aryl chlorides in Suzuki–Miyaura cross-coupling remains a long-standing challenge due to the inert nature of the C–Cl bond. Herein, we report the first nickel-catalyzed Suzuki–Miyaura cross-coupling of aryl chlorides under solvent-minimized, heated mechanochemical conditions. Employing liquid-assisted grinding (LAG) and thermal input, a broad range of electron-deficient and electron-rich aryl chlorides were successfully coupled with aryl boronic acids in under 1 hour. The methodology was translated to a twin-screw extrusion (TSE) process, enabling continuous production at scales up to 400 mmol and 65 g isolated product. This work demonstrates a sustainable, scalable strategy for C–C bond formation using readily available feedstocks, highlighting the synergy between nickel catalysis, mechanochemistry, and continuous flow processing.

Identifier
DOI https://doi.org/10.5522/04/29489774.v1
Related Identifier HasPart https://ndownloader.figshare.com/files/56024693
Related Identifier HasPart https://ndownloader.figshare.com/files/56024696
Related Identifier HasPart https://ndownloader.figshare.com/files/56024699
Related Identifier HasPart https://ndownloader.figshare.com/files/56024702
Related Identifier HasPart https://ndownloader.figshare.com/files/56024705
Related Identifier HasPart https://ndownloader.figshare.com/files/56024708
Related Identifier HasPart https://ndownloader.figshare.com/files/56024711
Related Identifier HasPart https://ndownloader.figshare.com/files/56024714
Related Identifier HasPart https://ndownloader.figshare.com/files/56024717
Related Identifier HasPart https://ndownloader.figshare.com/files/56024720
Related Identifier HasPart https://ndownloader.figshare.com/files/56024726
Related Identifier HasPart https://ndownloader.figshare.com/files/56024729
Related Identifier HasPart https://ndownloader.figshare.com/files/56024735
Related Identifier HasPart https://ndownloader.figshare.com/files/56024738
Related Identifier HasPart https://ndownloader.figshare.com/files/56024741
Related Identifier HasPart https://ndownloader.figshare.com/files/56024744
Related Identifier HasPart https://ndownloader.figshare.com/files/56024747
Related Identifier HasPart https://ndownloader.figshare.com/files/56024750
Related Identifier HasPart https://ndownloader.figshare.com/files/56024753
Related Identifier HasPart https://ndownloader.figshare.com/files/56024756
Related Identifier HasPart https://ndownloader.figshare.com/files/56024759
Related Identifier HasPart https://ndownloader.figshare.com/files/56024762
Related Identifier HasPart https://ndownloader.figshare.com/files/56024765
Related Identifier HasPart https://ndownloader.figshare.com/files/56024768
Related Identifier HasPart https://ndownloader.figshare.com/files/56024771
Related Identifier HasPart https://ndownloader.figshare.com/files/56024774
Related Identifier HasPart https://ndownloader.figshare.com/files/56024777
Related Identifier HasPart https://ndownloader.figshare.com/files/56024780
Related Identifier HasPart https://ndownloader.figshare.com/files/56024783
Related Identifier HasPart https://ndownloader.figshare.com/files/56024789
Related Identifier HasPart https://ndownloader.figshare.com/files/56024792
Related Identifier HasPart https://ndownloader.figshare.com/files/56024795
Metadata Access https://api.figshare.com/v2/oai?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:figshare.com:article/29489774
Provenance
Creator Raby Buck, Sarah; Browne, Duncan L. (ORCID: 0000-0002-8604-229x); Ingram, Katherine; Mattioli, Renan Rodini ORCID logo; Pastre, Julio (ORCID: 0000-0001-9972-425x); Bolt, Robert
Publisher University College London UCL
Contributor Figshare
Publication Year 2025
Rights https://creativecommons.org/publicdomain/zero/1.0/
OpenAccess true
Contact researchdatarepository(at)ucl.ac.uk
Representation
Language English
Resource Type Dataset
Discipline Chemistry; Natural Sciences