Supplementary files of research article "Photoswitchable Active Esters for the Control of Amide Bond Formation with Light". This research paper describes the preparation of patterned polymeric films controlled with two colors of light using photoswitchable crosslinkers through amide bond formation.
Bruker Topspin, 4.1.1 or higher
MestReNova, 12.0.0 or higher
OriginPro, 8.1 or higher
Universitat Autònoma de Barcelona. Grup d’Electroquímica, Fotoquímica i Reactivitat Orgànica (GEFRO).
METHODOLOGICAL INFORMATION
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Description of methods used for collection-generation of data:
NMR spectra: recorded on Bruker DPX250 (250 MHz for 1H), BRUKER 300 MHz AscendTM (300 MHz for 1H), DPX360 (360 MHz for 1H), AvanceIII 400NB (400 MHz for 1H) and Bruker System 600 Ascend LH (600 MHz for 1H) spectrometers.
IR spectrum: recorded on Bruker Tensor 27 Golden Gate spectrometer with a diamond tip.
MS spectrum: recorded on Bruker Esquire 3000+ spectrometer using ESI and timsTOF Pro 2 spectrometer using ESI.
UV-Vis spectra: recorded on Agilent HP 8453 spectrophotometer using 1 cm quartz cuvettes.
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Methods for processing the data:
NMR, IR, MS, SEC and image data are presented raw, UV-Vis spectra are presented after baseline substraction.
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Instrument- or software- specific information needed to interpret the data:
NMR spectra: Bruker Topspin 4.1.1 or higher, or MestReNova 12.0.0 or higher.
IR spectrum: OriginPro 8.1 or higher, or any other graphic representation program, such as Microsoft Excel.
MS spectrum: Adobe Acrobat Reader.
UV-Vis spectra: OriginPro 8.1 or higher, or any other graphic representation program, such as Microsoft Excel.
Other data: OriginPro 8.1 or higher, or any other graphic representation program, such as Microsoft Excel.
; Marco, Arnau