The dataset contains solid-state Nuclear Magnetic Resonance (NMR) recordings at 500 MHz from ~25 mg samples of 1-palmitoyl-2-oleoyl-sn-glycero-3-phosphocholine (POPC) in lamellar phase prepared at different hydration states (from 10 mass % to 50 mass %).
For every sample we put R-type proton-detected local field (R-PDLF) recoupling experiments recorded with magic angle spinning (MAS) at 5 kHz. This type of experiment allows us to extract the absolute values of order parameters of every C-H bond. We also put 31P spectrum at both 0Hz and 5kHz spinning to verify the lipid phase state. Most of samples contains also recordings of 13C spectra recorded with high repetition number.
Methodology is described in ReadMe in details.
TopSpin, 3.6.3