Simultaneous Raman and INS studies of cryolite Na3[AlF6].

DOI

Cryolite (Na3[AlF6], sodium hexafluoroaluminate) is a mineral with an unusual use: as the molten salt it is used as a solvent for aluminium oxides in the electrolytic refining of aluminium from its ores. The nature of the liquid phase is controversial with [AlF6]3-, [AlF5]2-, [AlF4]- and F- ions claimed to be present. The solid state has been much less studied. In principle, the low symmetry found in the low temperature phase, should remove all degeneracies and allow all the modes to be observed. However, only the Raman modes and the infrared active bending mode have been observed and there is no information on the whole body motions. The aim of this proposal is to observe all of the modes of cryolite by a simultaneous combination of Raman and INS spectroscopies.

Identifier
DOI https://doi.org/10.5286/ISIS.E.44927049
Metadata Access https://icatisis.esc.rl.ac.uk/oaipmh/request?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:icatisis.esc.rl.ac.uk:inv/44927049
Provenance
Creator Professor Stewart Parker
Publisher ISIS Neutron and Muon Source
Publication Year 2017
Rights CC-BY Attribution 4.0 International; https://creativecommons.org/licenses/by/4.0/
OpenAccess true
Contact isisdata(at)stfc.ac.uk
Representation
Resource Type Dataset
Discipline Chemistry; Natural Sciences; Physics
Temporal Coverage Begin 2013-12-05T00:00:00Z
Temporal Coverage End 2014-08-18T06:16:04Z