Particulate fucoidan concentrations during 24-days of incubations in mesocosm experiments with brown algae

DOI

Six mesocosm experiments with specimens of Fucales or Laminariales were conducted across six georegions (3 mesocosms with brown algae, 3 mesocosms without brown algae). Incubations lasted 24 days, followed by a year-long monitoring of incubation water. During the first 12 days, brown algae were maintained in mesocosms adjacent to control mesocosms, with 1 L of water sampled every second day. Half of the mesocosm water was replaced with fresh seawater after each sampling. Environmental conditions and primary productivity of specimens was recorded during the incubation. After 12 days, specimens were removed and incubation continued for another 12 days, maintaing the same sampling routine. At the end of the 24 day- incubation period, long-term monitoring was set-up with 6-10L of incubation water in two different conditions: one exposed to a controlled light cycle at 20°C, the second set in darkness at 4°C with added nutrients (40 µM NO3- and 3µM PO43-). Additional water samples were collected along transects extending from near-shore brown algae poplulations. Water samples were filtered over pre-combusted GFF filters (450°C, 4.5h), and both the filtrate and filters were analysed for dissolved organic carbon (DOC), particulate organic carbon (POC). Fucoidan was quantified in size-selected (>1kDa) fraction and size- and charge-selected (> 1kDa and negative charged fraction purified with anion exchange chromatography) fractions through monosaccharide quantification after acid-hydrolysis (100°C, 24h) using HPAEC-PAD, according to Engel and Händel, 2011. Intact polysaccharides were detected using structure-sensitive monoclonal antibodies (Torode et al., 2015; Vidal-Melgosa et al., 2021). Microbial cells were quantified using DAPI-cell staining and counting. Semi-quantitative measurements of particulate fucoidan were performed via acid hydrolysis of GFF fitler pieces, followed by monosaccharide analysis via HPAEC-PAD. Sedimented particles to bottom of mesocosms were scooped out on day 24 for monosaccharide analysis and BAM1 antibody binding specific to fucoidan.

Identifier
DOI https://doi.pangaea.de/10.1594/PANGAEA.980721
Related Identifier IsPartOf https://doi.pangaea.de/10.1594/PANGAEA.980715
Related Identifier References https://doi.org/10.1016/j.marchem.2011.09.004
Related Identifier References https://doi.org/10.1371/journal.pone.0118366
Related Identifier References https://doi.org/10.1038/s41467-021-21009-6
Metadata Access https://ws.pangaea.de/oai/provider?verb=GetRecord&metadataPrefix=datacite4&identifier=oai:pangaea.de:doi:10.1594/PANGAEA.980721
Provenance
Creator Hellige, Inga ORCID logo; Buck-Wiese, Hagen ORCID logo; Thomson, Timothy; White, Lydia; Kajee, Mohammed; Potin, Dan; Salgado Murillo, Beatriz; Lloyd, C Chad; Ghobrial, Sherif; Bligh, Margot ORCID logo; Uth, Catharina; Baiko, Dariya; Philippi, Miriam ORCID logo
Publisher PANGAEA
Publication Year 2025
Funding Reference Federal Ministry of Education and Research https://doi.org/10.13039/501100002347 Crossref Funder ID 03F0896E https://foerderportal.bund.de/foekat/jsp/SucheAction.do?actionMode=view&fkz=03F0896E DAM CDRmare - sea4soCiety, University of Bremen
Rights Creative Commons Attribution 4.0 International; Data access is restricted (moratorium, sensitive data, license constraints); https://creativecommons.org/licenses/by/4.0/
OpenAccess false
Representation
Resource Type Dataset
Format text/tab-separated-values
Size 3116 data points
Discipline Earth System Research
Spatial Coverage (-71.634W, -37.671S, 176.167E, 59.844N); South Pacific Ocean; North Atlantic Ocean; English Channel; Baltic Sea; South Atlantic Ocean
Temporal Coverage Begin 2022-01-28T17:00:00Z
Temporal Coverage End 2022-10-31T08:00:00Z