Towards Understanding Lignin Solubility in Protic Ionic Liquids

DOI

A current key road block to the economic viability of a biorefinery is the inability to cost effectively separate biomass into lignin and cellulose. It has recently been reported that protic ionic liquids (PILs) can be used to extract lignin from lignocellulose to produce lignin-rich and cellulose-rich streams. However, the means by which the PIL (selectively) solubilises the lignin has not been explored. In this project we will elucidate interactions which promote the solubility of guaiacol (2-methoxyphenol) and hydroquinone (4-hydroxy-3-methoxybenzaldehyde) in ethylammonium nitrate (EAN) and ethylammonium hydrogen sulphate (EAHS). Comparison of the PIL nanostructures with and without added solute, and the favoured orientations of ions around the model solutes, will reveal the ion ¿ solute interactions that are key to the solubility of lignin-like materials in PILs.

Identifier
DOI https://doi.org/10.5286/ISIS.E.61781414
Metadata Access https://icatisis.esc.rl.ac.uk/oaipmh/request?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:icatisis.esc.rl.ac.uk:inv/61781414
Provenance
Creator Professor Rob Atkin; Ms Samila McDonald; Professor Greg Warr; Ms Haihui Joy Jiang; Dr Silvia Imberti; Dr Blake Simmons
Publisher ISIS Neutron and Muon Source
Publication Year 2018
Rights CC-BY Attribution 4.0 International; https://creativecommons.org/licenses/by/4.0/
OpenAccess true
Contact isisdata(at)stfc.ac.uk
Representation
Resource Type Dataset
Discipline Chemistry; Natural Sciences
Temporal Coverage Begin 2015-06-29T08:00:00Z
Temporal Coverage End 2015-07-04T08:00:00Z