Revealing electrochemically activated polymer infiltration into thick cathodes in solid-state batteries

DOI

Solid-state batteries are next-generation energy storage technologies that replace flammable electrolyte with safer solid counterparts. Yet, inorganic solid electrolytes suffer contact loss upon cathode volume changes during charge/discharge, limiting electrochemical performances. Polymer electrolytes are considered contact loss-free, especially when they are used above melting temperatures. We developed a new polymer that excels at room temperature. Interestingly, our preliminary results at ID31 beamline contest the common belief about polymers: it cannot infiltrate through the cathode under external mechanical pressure; yet the infiltration is strongly enhanced after the first charge/discharge cycle. Here we propose to use sub-µm X-ray CT at ID16B to resolve this puzzle, by finding out when and how polymer permeates in the electrode microstructure. The electrochemically activated infiltration mechanism may provide insights to design polymer electrolytes and solid-state batteries.

Identifier
DOI https://doi.org/10.15151/ESRF-ES-1584277816
Metadata Access https://icatplus.esrf.fr/oaipmh/request?verb=GetRecord&metadataPrefix=oai_datacite&identifier=oai:icatplus.esrf.fr:inv/1584277816
Provenance
Creator Qing WANG ORCID logo; Julie VILLANOVA; Gustavo Adolfo PINZON FORERO ORCID logo; Francesco BERNASCONI ORCID logo
Publisher ESRF (European Synchrotron Radiation Facility)
Publication Year 2027
Rights CC-BY-4.0; https://creativecommons.org/licenses/by/4.0
OpenAccess true
Representation
Resource Type Data from large facility measurement; Collection
Discipline Particles, Nuclei and Fields