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Single-crystal neutron diffraction study of sucrose at high pressure.
In the context of expanding the sample environments available for experiments on the SXD instrument, the Paris-Edinburgh press recently developed on PEARL offers the possibility... -
Evaluation of a low temperature solid-solid phase transition of 4?-hydroxyace...
This dataset has no description
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Radiation induced hydrogen abstraction - A combined X-ray and neutron diffrac...
X-ray induced radiation damage drastically limits the structural information accessible in diffraction experiments from macromolecules at 3rd generation synchrotrons. Relatively... -
A unique borohydride bridged dimer of Ni(I)
The reaction of Ni(6-Mes)(PPh3)Br (6-Mes = bis(1,3-(2,4,6-trimethylphenyl)imidazol-2-ylidene) with 2.5 equivalents of NaBH4 leads to formation of product characterised as... -
Crystal Structure of Green Dioptase
This dataset has no description
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Long-range cationic ordering in metal-organic perovskite solid solutions
The structure of the metal guanadinium formates is analogous to perovskite; the Cu compound is of particular interest as a potential multiferroic. We have recently demonstrated... -
Combined neutron and X-ray single-crystal diffraction studies of selected 2-p...
Hydrozones and their metal complexes exhibit subtle redistribution of electron density as a function of substitution, type of the metal center and intermolecular interactions.... -
All-trans Retinal T=100K wtl=10 j:14,14
This dataset has no description
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Crystal structures of Na2MoO4.10H2O, Na2WO4.10H2O and Na2MnO4.10H2O.
Chemical substitution is a valuable technique for probing the behaviour of materials since this exerts a stress comparable in many respects to changes in pressure or... -
Anharmonic thermal motion of hydrogen atom(s)
This is a feasibility study of a possible influence of anharmonic thermal motion of hydrogen atom(s) on quantitative electron density distributions in single crystals of model... -
Multitemperature measurements of 2,6-diaminopurine monohydrate crystals
This dataset has no description
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Proton ordering and hydrogen bonding in the hydrous zinc phosphate hopeite, Z...
We request 4 days of beamtime on SXD in order to locate the protons and quantify their ordering within the structure of hopeite Zn3(PO4)2.4H2O. Hopeite is an important phase in... -
Determination of the crystal structure of CsNiCl3 and RbNiCl3 under hydrostat...
This dataset has no description
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Investigating the origin of thermochromism in N-salicylideneanilines
Anils, N-salicylideneanilines, display thermochromism, which is thought to involve an intramolecular proton shift, but to-date the structural changes postulated to occur during... -
Single-Crystal Neutron Diffraction Study on [U(C5Me5)2(H)(mu¿H)]2
To our knowledge, the length of the U¿H single bond has never been accurately measured, at least not in a molecular compound by single-crystal neutron diffraction. We currently... -
Elucidating the Structure of [(LaCl)Ti28O40(OEt)38(X)]; but what is X?
Metal-doped TiO2 have particular applications as in catalysis of a range of reactions as well as in luminescence materials. Our strategy is to make well-defined molecular TixOy... -
Structural characterization of a fully detuterated manganese Prussian Blue an...
The aim of this proposal is to perform a neutron diffraction determination of the first perdeuterated Mn-Prussian Blue (PB) analogue of composition: Mn(II)3 [Mn(III)(CN)6]2... -
Cation substitution in synthetic meridianiite (MgSO4.11H2O): site distributio...
MgSO4.11H2O (MS11) is the most highly hydrated phase in the binary MgSO4¿H2O system. Whilst lower hydrates in this system have end-member analogues containing alternative... -
Structure of TEA(TCNQ)2
This dataset has no description
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Crystal structure of mallardite, manganese sulfate heptahydrate
This dataset has no description
